Chemiolis - 2023-01-08
Support my channel with patreon: https://www.patreon.com/chemiolis in this video I am making Thiobenzoyl Chloride, which might be one of the few deep pink liquids at room temperature! Besides being pretty, it's also a (toxic) reagent for making Thionoesters. Followed paper: https://chemistry-europe.onlinelibrary.wiley.com/doi/abs/10.1002/chem.201904132
Glad to see Explosions&Fire has taught everyone the sins of yellow chemistry
Hah! Hah! I love working with fool’s gold!
And after learning how evil yellow chemistry is from E&F, he overtook his teacher and made cubane before him xD
Just got accepted into a university in Korea as a Chem major
Your videos made me love chemistry ❤️ 💙 💜
화이팅!
ladies and gentlemen, we got em
Just got into a PhD in chem at Korea too. Good luck in your studies
@Rafi Muhammad wow a PhD that's amazing 👏
Congratulations! I wish you the best of luck!
It looks the exact same as when I made it :D
Stalker ;-)
I wish someone would love me as much as Chemiolis loves his short path vacuum distillation apparatus.
he does not love it - he is trying his best to get a rotovap!
@@That_Chemist I'm using rotovaps during my pratical application courses in university. Literally one of the most useful things i've ever used.
It appears that Extractions&Ire is not alone in his fear of yellow chemistry lol.
That phase guessing gives me flashbacks to my crystal violet synthesis. Lamp standing next to the sep funnel and just hoping what you see is actually the layer
You had me going in the first half. I thought it was gonna be a one-pot synthesis. Then the extractions started.
Love the fact that you do a short demo using the new compound following the workup - really shows what it can do.
That Chemist wants to know your location
Thanks for the greatest to date organic chemistry videos content on the web.
I think my soul died a bit inside through that long and winding purification process, dear god
I like to watch the tiny stir bar dance around as it stirs near the end.
That looks awesome! Love your videos!
I like so much your channel, its the most motivational and the big masterpiece, regards master from 🇨🇱 Chile
Also want to recommend an IR camera for seeing phase separation (like the ones used for security). I was doing a caffeine extraction where the emulsion layer thickness was unclear, and the IR camera was able to see it perfectly. Food for thought
That would be really fucking cool. Sounds like a whole youtube channel but honestly it sound like a whole sub field of chemistry.
Amazing video with one of my favorite compounds. Thank you!
Also would be interesting to see some thionation reactions)
7:56 This is a wonderful shade of pink :)
I'm only 15 years old, so I don't know that much about chemistry, but it is interesting to me! Keep up the good work!
Amazing vids! Remind me of when i made thiobenzophenone. Pretty unstable sadly but have a amazing blue color!
Thank you kindly for helping me cleanse my system from all nasty yellow chemistry I've been exposed to lately. 😊
Beautiful! Usually organic compounds are so dull in appearance.
Little tip when doing extractions or column chromatography and having trouble seeing the layers or bands you can use a flash light behind the sep funnel shined at it and it makes it more distinct. May be helpful for improving quality. Enjoyed keep it up.
This was so pretty and interesting, thank you
I've been taught to always secure the canula with one hand when injecting solvents or chemicals. This is just as an added safety in case you excert too much pressure on the stopper. Like at 6:30, you wouldn't want the canula to pop off and spray thionyl chloride everywhere.
Well done!
I have no clue what i just watched but i was worth all the while
Pink chemistry is so good💕💕💕
Hey! Sulfur is one of my favorite elements, and along with chlorine, made me realize that I like yellow
chemiolis always got the craziest stir bars
Grignard reaction AND pink chemistry? What a time to be alive! 😁
I totally forgot that besides doing the chemistry you are responsible for camera work - those exposure comments reminded me of that
all of the non-chemistry parts of making chemistry videos actually make up like 90% of what we do
thats quite a unique substance,
Really entertaining.
At 6:38, why did you put on the stopper for a reaction that has gas as a product?
nice i did not know you could do the same thing with a carbon disulfide and grignard as carbondioxide learned somethin new great video
it usually needs to be the grignard btw - organolithiums attack at the sulfur of CS2 a lot of the time, so you get thiols through a cursed mechanism
Thios can be tricky. Liked that you used dry N2.
Super! Thank you very much! It is soluble in water?
"my bloody valentine - loveless" chemical doesn't exist it cannot hurt you
"my bloody valentine - loveless" chemical:
I've always wondered where to find tetrahydrofurant even considered distillation from PVC cleaner.. Seems ultra versatile and crucial for Grignard Reactions. Beautiful synthesis.
You can just straight order THF from Amazon or eBay. Also I would be careful about distillation because it can form explosive peroxides. There's also a few 3D printing supply stores that carry it for post-processing. from what I remember you shouldn't boil dry THF due to the peroxide contamination risk.
A pretty final product, with interesting reactions, and a long, satisfying purification process that I didn't have to do. Exactly what I needed after college classes today. Thanks! What's the catalytic mechanism of DMAP? Is it a helpful ligand in this reaction?
@@Correct_Opinion thanks!
"becose its not yellow"-giga chad
where do you buy the small square bottles with blue cap?
love the videos!!!!
Thanks! I bought them from Carl Roth
I remember in my 4th year undergrad qualitative organic class I dropped thionyl Chloride on the ground and we had to evacuate the lab.
No stench description?
Boy, with THAT sulphur Layout!
Oncebhad to deal with thiophenol....
Oof that burn on that chemist roast
👀
May i ask, what does dithiobenzoic acid smell like?
Chemiolis the GOATEST
the chemical slayed
Now is the pink substance made in the film flammable
fantastic
Shots fired at "That Chemist"
@FUZxxl - 2023-01-08
Not yellow is the best motivation for making a chemical.
@mgancarzjr - 2023-01-08
Extractions and Ire taught us well.
@lukassorowka2672 - 2023-01-09
or TAR
@ackbarreserve - 2023-01-09
@@lukassorowka2672 delicious, delicious TAR
@user-sj3pc7ww1x - 2023-01-09
😂🤣
@Aochso - 2023-01-16
Whats up with this yellow chemistry meme? Saw it all over extraction&ire's channel