> chemistry > oxydants > perchloric-acid > hclo4-from-nh4clo4-no-distillation-laboratory-of-liptakov

HClO4 ........(from NH4ClO4)

Laboratory of Liptakov - 2019-04-06

Exist a lot methodes of prepare HClO4. But this provide pure product in easy way and short  time.
HClO4 we usually not needed. We need  only his salts. Especially NH 4 ClO 4. Here is the procedure reversed. HClO4 is produced from NH4ClO4. Only very poorly soluble AP remains in solution. When cooled to -18 Celsius, 99.9% AP is precipitated.

Feed Me - 2019-04-06

Great content once again. Thank you Dr 😍

Science 007 - 2019-04-06

Doc you always suprise me with new stuff I LOVE IT!

Laboratory of Liptakov - 2019-04-06

Well, Mad Acid.....:-)

Chris Maris - 2019-04-08

nice patent with the heat gun. 💪
once again, great stuff.
Can you upload the "nitrocellulose stabilizer" again? I don't remember the analogy between acetone an ammonium. I don't find it. thnx a lot Doc

Briant W - 2019-04-07

Thank you Dr. Please make more videos!

luke craft - 2019-12-15

Could you please make a video on this acid on fruits/sponges bro I've only just been learning about these super acids and anything stronger then chlorosulfonic acid is impossible to find any sort of videos on and that stuff was pretty impressive as the weakest super acid

mark yisser - 2021-04-24

Wow!. All with simple instruments.
I'm a fan...

Make more.

Waylen Edge - 2019-04-07

Very nice work doc!

[TQL 120%] - 2019-04-06

ОГО! Перхлорная кислота собственной персоной! Это лайк.

Laboratory of Liptakov - 2019-04-06

На YouTube очень мало Перхлорной кислоты....:-)

Chemist Kid - 2019-04-06

Lower pH level than sulfuric acid right?

Laboratory of Liptakov - 2019-04-07

Yes, but HClO4 is much friendly during manipulation. No steam gases at open glass jar.

MysteriusBhoice - 2021-04-06

going to make HClO4 using another way.
dissolve CaCl2 and NaClO4 in weight ratio of 1:2 in minimal amount of water.
add concentrated H2SO4 slowly into this heated solution.
filter cloudy precipitate with polythene strainer not paper.
distill the acid out

Laboratory of Liptakov - 2022-02-14

This is certainly a better method. But only for the one who has a distiller. The Adams method uses only one beaker. // Let's do things as simply as possible // Albert Einstein.

MrMistery - 2020-05-08

Why not just desolve a perchlorate salt in sulfiric acid, I mean it would be a lot easier

Chemistry'sCuriosities Cannagorilla - 2019-08-09

Why not just use sodium perchlorate and acidify that boil down filter out salts?

Prathamesh Zingade - 2021-09-16

Just wow

Enrique Gijon - 2020-03-29

No sabemos nada de usted ! se encuentra usted bien? va todo bien ?,un fuerte abrazo DR

Laboratory of Liptakov - 2020-11-07

All is OK

Eimantas a - 2019-04-06

Instant like !

becam mac - 2019-04-09

How to Prepare Perchloric Acid from Potassium Perchlorate

Si da sci guy inc - 2019-04-06

grand old boy, grand!

science_and_anonymous - 2019-04-09

YES!!! AMATEUR EXPLOSIVE HOLY GRAIL

Laboratory of Liptakov - 2019-04-09

OK, Holy Grail of all amateur is here. And will tetsted.....:-)

Chemistry'sCuriosities Cannagorilla - 2019-08-09

@Laboratory of Liptakov we love ya man

Брюс Ли - 2019-08-14

Супер

Jérôme Schmitz - 2021-01-05

This is slightly crazy

Accipiter Nisus - 2019-04-06

Nice edit hahahaha

ProPyroPower - 2019-04-06

where you doing a facereveal? 5:19 - hello sir

Chemistry'sCuriosities Cannagorilla - 2019-08-09

Where did you think you saw his face?

Science 007 - 2019-04-06

But cant you also make it with just Perchlorates and Sulfuric acid?

Laboratory of Liptakov - 2019-04-06

Exist a lot methodes of prepare HClO4. But this provide pure product in easy way and short time.

Meneltir - 2019-04-06

In that method you'd have to distill it, which is both extremely difficult and dangerous.

Science 007 - 2019-04-08

Ok thanks

MysteriusBhoice - 2021-04-06

@GMC Labs distilling HClO4 under vacuum you need NaOH trap or your vacuum pump oil will turn into organic perchlorates and blow up your pump