Cubane synthesis - Extractions&Ire
cubane-synthesis-
Many interesting techniques in this series : recrystalizations, purifications, TLCs with various detection methods (permanganate, iodine, UV, vanillin), contamination mitigation, quite cold temperatures, reaction times, decomposition, photochemistry, protection/deprotection, water-free techniques, tar management...
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Project plan: Cubane synthesis - Extractions&Ire
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Synthesising Cyclopentanone through Catalytic Decarboxylation of Adipic acid - Extractions&Ire
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Cubane Episode 2 - Cyclopentanone Ketal [failure : aldol condensation] - Extractions&Ire
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Cubane Episode 3 - Vacuum Distillation for the Ketal? [failure] - Extractions&Ire
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Mastering the Ketal Synthesis [or how to avoid aldol cond.] - Cubane Episode 4 - Extractions&Ire
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Cubane Ep 5 - Dioxane and Bromine [chlorine-free Br2 with H2O2] - Extractions&Ire
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Bromination of the ketal - Cubane Episode 6 - Extractions&Ire
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The Diels-Alder - Making Cubane Episode 7 - Extractions&Ire
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Cubane Ep 8 - Deprotection Time! Diketal to monoketal [in heterogeneous mixture, HCl]. TLC stuff. - Extractions&Ire
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Cubane Ep 9 - *Actually* forming the MonoKetal. Amazing NMR results - Extractions&Ire
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Cubane Ep 10 - Ultraviolet Cage Creation [failure] - Extractions&Ire
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Cubane Ep 11 - More UV Nightmares [failure, more TLC nightmares] - Extractions&Ire
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Cubane Ep 12 - Magical deep UV LEDs [failure] - Extractions&Ire
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Cubane Ep 13 - The PhotoFridge [failure] - Extractions&Ire
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A slightly new cube plan... [UV sensitization, litterature review, progress by others] - Cubane Ep 14 - Extractions&Ire
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I lost the cubane race (Still going though!) [new plan : no monoketal intermediate, doing the photoreaction directly on the diketone; resynthesis and purification of reagents] - Cubane Ep. 15 - Extractions&Ire
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Cubane synthesis - Chemiolis