Répertoire de liens : Chimie

Physico-chimie
physico-chimie
- Azeotrope
  https://en.wikipedia.org/wiki/Azeotrope
- Explanation of what happens when hard water is heated.
  https://woelen.homescience.net/science/chem/exps/bicarbonate/index.html
- Theoretical Plates Required to Separate Mixtures, Hive Methods Discourse
  https://chemistry.mdma.ch/hiveboard/methods/000358631.html
- Chemistry of the Cocktail: The Physics of Batch Column Stills and Bubble Plates
  http://cocktailchem.blogspot.com/2019/01/the-physics-of-batch-column-stills-and.html
- Nice small text on liquid-liquid extraction theory - ScienceMadness
- The Cinnamaldehyde Clock - NileRed
- Screaming gallium when reacting with bromine in water - ChemicalForce
- Ammonia Fountain and Balloon - Periodic Videos
- Make Paramagnetic Fluid ("Parafluid") MnNO3 in DCM - NurdRage
- Make Quantum Dots (Cadmium Selenide Type) - NurdRage
- Why is chemistry unpredictable? - Chemistry Stack Exchange
  https://chemistry.stackexchange.com/questions/141689/why-is-chemistry-unpredictable
- Descaling magnetic water treatment
  descaling-magnetic-water-treatment
  - Effect of magnetic water treatment on calcium carbonate precipitation: Influence of the pipe material - Alimi, 2009
  - Magnetic water treatment - Coey, 2000
  - A critical review of the application of electromagnetic fields for scaling control in water systems: mechanisms, characterization, and operation
    https://www.nature.com/articles/s41545-020-0071-9.pdf
- Charbon actif
  charbon-actif
  - Tailoring Activated Carbons for Efficient Downstream Processing Selective Liquid‐Phase Adsorption of Lysine - Deischter 2020 [good info on different types of activated charcoal, surface groups, variable hydrophobicity, selectivity...]
  - Tailoring Activated Carbons for Efficient Downstream Processing Selective Liquid‐Phase Adsorption of Lysine - Suppl. Info.
- Reaction between Gallium and Bromine in water : it's alive ! - ChemicalForce
Chimie générale
chimie-générale
- Cours de chimie L1->M2 pour ingés - perso.numericable.fr/chimorga
  http://perso.numericable.fr/chimorga/niveauM1.php
- Animations de réactions chimiques au niveau moléculaire
  animations-de-réactions-chimiques-au-niveau-moléculaire
  - SPRINT: automatic discovery of chemical reactions - Fabio Pietrucci
  - Simulation of Hydrogen burning under 100,000,000x microscope (2H2+O2=2H2O) - MEL Science
- Click chemistry
  https://en.wikipedia.org/wiki/Click_chemistry
Théorie inorganique
théorie-inorganique
- Diagramme de Frost
  https://fr.wikipedia.org/wiki/Diagramme_de_Frost
- Relative Strengths of Acids and Bases - Chemistry LibreTexts
  https://chem.libretexts.org/Courses/CSU_San_Bernardino/CHEM_2100%3A_General_Chemistry_I_(Mink)/14%3A_Acid-Base_Equilibria/14.03%3A_Relative_Strengths_of_Acids_and_Bases
- Electride
  https://en.wikipedia.org/wiki/Electride
- Iron solutions and tests - Woelen
  https://woelen.homescience.net/science/chem/solutions/fe.html
Théorie organique
théorie-organique
- Nucleophilic substitution
  https://en.wikipedia.org/wiki/Nucleophilic_substitution
- Arrow pushing
  https://en.wikipedia.org/wiki/Arrow_pushing
- Ethylene oxide : de très nombreuses réaction d'addition...
  https://en.wikipedia.org/wiki/Ethylene_oxide
- Synthesis Workshop: Demystifying the Soai Reaction (making an homochiral compound from non-chiral compounds through non-linear autocatalytic reactions) with Dr. Soumitra Athavale
- The Williamson Ether Synthesis – Master Organic Chemistry
  https://www.masterorganicchemistry.com/2014/10/24/the-williamson-ether-synthesis/
- Claisen condensation
  https://en.wikipedia.org/wiki/Claisen_condensation
- Ketonic decarboxylation
  https://en.wikipedia.org/wiki/Ketonic_decarboxylation
- Epoxidation of Alkenes with Peracids
  http://www.chemgapedia.de/vsengine/vlu/vsc/en/ch/2/vlu/oxidation_reduktion/epxo_per_1.vlu.html
- Oxidations : Peracetic acid
  https://www.organic-chemistry.org/chemicals/oxidations/peracetic-acid.shtm
- Prins reaction (addition to an alkene)
  https://en.wikipedia.org/wiki/Prins_reaction
- Nucleophilicity vs. Basicity – Master Organic Chemistry
  https://www.masterorganicchemistry.com/2012/06/06/nucleophilicity-vs-basicity/
- Fischer–Tropsch process : building liquid hydrocarbons from syngas/C1
  https://en.wikipedia.org/wiki/Fischer%E2%80%93Tropsch_process
- Élimination de Hofmann
  https://fr.wikipedia.org/wiki/%C3%89limination_de_Hofmann
- Hückel method
  https://en.wikipedia.org/wiki/H%C3%BCckel_method
- Réaction de Réformatski
  https://fr.wikipedia.org/wiki/R%C3%A9action_de_R%C3%A9formatski
Agents acylants, Acylations
agents-acylants
- Anhydride acétique
  anhydride-acétique
  - Acetic anhydride preparation
    http://www.sciencemadness.org/talk/viewthread.php?tid=9
  - Acétate de sodium + Monochlorure de soufre -> Anhydride Acétique
    https://www.erowid.org/archive/rhodium/chemistry/anhydrides.html
  - Acetic Anhydride from Vinegar: The Sulfur Chloride Route [easy !] - LabCoatz
  - Preparation of acetic anhydride from acetyl chloride and acetate - THYZOID LABORATORIES
- Chlorure d'acyle
  https://fr.wikipedia.org/wiki/Chlorure_d%27acyle
- Ethenone
  https://en.wikipedia.org/wiki/Ethenone
- Synthesis of p-Methylacetophenone : Friedel-Crafts acylation of toluene with acetic anhydride - Corrosive Chemistry
- Friedel Crafts acylation of toluene - Barnali Mondal
Agents alkylants, Alkylations
agents-alkylants
- Iodomethane / Methyl iodide
  https://en.wikipedia.org/wiki/Iodomethane
- Organolithium reagent
  https://en.wikipedia.org/wiki/Organolithium_reagent
- Methyllithium
  https://en.wikipedia.org/wiki/Methyllithium
- Dimethyl carbonate
  https://en.wikipedia.org/wiki/Dimethyl_carbonate#Methylating_agent
- Dimethyl sulfate
  https://en.wikipedia.org/wiki/Dimethyl_sulfate
- Alkyl tosylate (MeTs...)
  methyl-tosylate-mets
  - Safer but milder alkylating agent (still carcinogenic)
  - n-BUTYL p-TOLUENESULFONATE - OrgSyn
    http://www.orgsyn.org/demo.aspx?prep=cv1p0145
  - Methyl tosylate: finally OTC! [+ its use for many many methylations !] - The Hive
    https://chemistry.mdma.ch/hiveboard/novel/000417550.html
  - Preparation of methyl tosylate - Sciencemadness
    http://www.sciencemadness.org/talk/viewthread.php?tid=11004
- Methylation with methanal and Zn metal (Eschweiler–Clarke variant)
- Eschweiler–Clarke reaction
  https://en.wikipedia.org/wiki/Eschweiler%E2%80%93Clarke_reaction
- Synthèse de la N,N-diméthylbenzylamine - Chimie Organique de A à Z
  http://chimieorganique-jeanlouis-migot.over-blog.com/2020/05/179-synthese-de-la-2-3-diphenylquinoxaline.html
Chemiluminescents & Fluorescents
chemiluminescents
- Réactions chimioluminescentes - scienceamusante.net
  http://wiki.scienceamusante.net/index.php/R%C3%A9actions_chimioluminescentes
- Peroxyoxalates
  peroxyoxalates
  - Peroxyoxalates (mechanism)
    https://en.wikipedia.org/wiki/Peroxyoxalate
  - Diphenyl oxalate / Cyalume (quite green and simple but inefficient)
    https://en.wikipedia.org/wiki/Cyalume
  - Synthèse TCPO/DNPO
    http://wiki.scienceamusante.net/index.php/TCPO/synth%C3%A8se
  - DNPO [2,4-dinitrophenol]
    https://en.wikipedia.org/wiki/Bis(2,4-dinitrophenyl)_oxalate
  - Divanillyl oxalate paper (greener alternative)
  - MCPO [methyl salicylate]
    https://en.wikipedia.org/wiki/MCPO
  - MCPO : methyl salicylate-based chemiluminescent, greener alternative to the trichlorophenol-based TCPO - NileRed
  - CPPO [2-carbopentoxy-3,5,6-trichlorophenol]
    https://en.wikipedia.org/wiki/Bis(2,4,5-trichlorophenyl-6-carbopentoxyphenyl)oxalate
  - Dimethyl Oxalate - Doug's Lab [can replace oxalyl chloride ??]
  - PCPO : Determination of absolute chemiluminescence quantum yields for reactions of bis-(pentachlorophenyl) oxalate, hydrogen peroxide and fluorescent compounds
  - Chemiluminescent materials (may tests of oxalates, in many solvants, concentrations...) - Naval research report, 1965
  - Vapor Activated Glow Stick - NurdRage
  - Demonstrations of Chemiluminescence - Frank McCapra
  - All Eyes on Visible Light Peroxyoxalate Chemiluminescence Read-Out Systems - Delafresnaye, 2019
  - Make Glow Sticks of different colors - NurdRage
  - How to make TCPO - NurdRage
  - Luminol and TCPO Chemiluminescence
    https://www.shsu.edu/~chm_tgc/JPPdir/JPP1999/
- R.O.S. - Singlet O2 luminescence via H2O2 + Ca(ClO)2 - Rhodanide
- Synthesis and Verification of 9,10-Diphenylanthracene and Its Utility as a Fluorescer in a Peroxyoxalate Chemiluminescence System. An Organic Laboratory Project Integrating Synthesis with Fluorescence and Chemiluminescence - Zhi 2000
- How Fluorescence Works - tricks and remarks with fluo dyes, abs/em spectra, applications... - NurdRage
- How to Make Fluorescein (Fluorescent Dye) (phenolphtalein reaction) - NurdRage
- Make Blue Smash-Glow Crystals (Tryphenylphosphinebis(pyridine)thiocyanatocopper(I)) (Triboluminescence Demonstration) - NurdRage
- Make Red Smash-Glow crystals (Europium Tetrakis (Dibenzoylmethane)Triethylammonium) - NurdRage
- Make a Color Changing Glow Stick : using the unstability of Rhodamine B - NurdRage
- Make Luminol - The Complete Guide - NurdRage
- Make Flowers Glow In The Dark (with highlighter fluid and UV light) - NurdRage
- Phosphorescents
  phosphorescents
  - Make Green glow-in-the-dark powder (strontium, europium and dysprosium based) - NurdRage
  - Make Blue glow-in-the-dark powder (calcium, europium and dysprosium based) - NurdRage
Tests/Indicators
tests
- Testing for boron with curcumin (turmeric) - TheHomeScientist
- Forensic Presumptive Drug Testing I - TheHomeScientist
- Testing for Alkaloids with Dragendorff Reagent - TheHomeScientist
- Salicylate determination with visual colorimetry - TheHomeScientist
- Synthesis of Dicinnamalacetone - Corrosive Chemistry
- Titration of vitamin C with iodometry
- Make Potassium Rhodizonate (for lead testing) - NurdRage
- Test for Lead Using Potassium Rhodizonate - NurdRage
- Rhodizonic acid
  https://en.wikipedia.org/wiki/Rhodizonic_acid
Acides
acides
- Acide chlorhydrique
  acide-chlorhydrique
  - Make Hydrochloric Acid (bisulfite/NaCl method) - NurdRage
- Acide formique (methanoic acid)
  acide-formique
- Acide acétique (ethanoic acid)
  acide-acétique
  - Concentrated Acetic Acid from H2SO4 and sodium acetate - Doug's Lab
- Acide propanoïque (propionic acid)
  acide-propanoïque-propionic-acid
  - Propionate (de sodium, calcium) sur Aliexpress/eBay comme food preservative, pas cher
  - Propionic acid -> Production
    https://en.wikipedia.org/wiki/Propionic_acid#Production
  - Make Propionic Acid by the Haloform Reaction (MEK+bleach) - NurdRage
    make-propionic-acid-by-the-haloform-reaction-mek-bleach-nurdrage
    
    Make chloroform by the haloform reaction - NurdRage
    
    Make Propionic Acid by the Haloform Reaction (MEK+bleach) - NurdRage
- Acide butanoïque (butyric acid)
  acide-butanoïque-butyric-acid
  - Butyrate salts sold as dietary supplement
  - How to make Butyric Acid (Grignard Reaction, from bromopropane) - NileRed
  - How to make Butyric Acid (Oxidation of butanol) - NileRed
  - Butyric acid -> Microbial biosynthesis
    https://en.wikipedia.org/wiki/Butyric_acid#Microbial_biosynthesis
- p-Toluenesulfonic Acid
  p-toluenesulfonic-acid
  - Make p-Toluenesulfonic Acid - NurdRage
  - Sulfonation: p-Toluenesulfonic Acid - Doug's Lab
  - Synthesis of p-Toluenesulfonic Acid Monohydrate - UC235
- Magic Acid: Fluorosulfonic acid + Antimony pentafluoride - ChemicalForce
Bases
bases
- Preparation of Sodium Methoxide CH₃ONa - AllChemystery
- Methoxide
  https://en.wikipedia.org/wiki/Methoxide
- Ammonia
  ammonia
  - Ammonia Generator (Ammonium salt + NaOH) - Doug's Lab
  - Preparing conc. aqueous ammonia, Ammonia gas generator - ChemPlayer
  - Make Concentrated Ammonia - NurdRage
  - Anhydrous ammonia : decomposition of ammonium persulfate (2x NH3) ?; decomposition of ammonium carbonate (2x NH3) + water scrubber (NaOH pellets?); decomposition of ammonium phosphate (3x NH3); decomposition of ammonium sulfate (2x NH3)
  - Liquefying Ammonia NH3 Gas from ammonia water with a compressor - Elias Experiments
Halogènes
halogènes
- Chlore gazeux
  chlore-gazeux
  - Chloroalkali mercury cell - Cody's Lab
  - Electrolysis of molten zinc chloride -> zinc metal and chlorine
    https://edu.rsc.org/experiments/electrolysis-of-molten-zinc-chloride/826.article
- Dibrome
  dibrome
  - Preparation of Bromine - Doug's Lab
  - How to make bromine (Persulfate-method, without sulfuric acid or chlorine) - Experimental Chemistry
Oxydants
oxydants
- Oxidizer Tierlist - That Chemist
- Making (and reacting) Chromyl chloride - NileRed
- Chromyl Chloride - Doug's Lab
- Manganese heptoxide - NileRed
- Dealing with my manganese heptoxide waste - NileBlue
- Chemical Thunderstorm in a Beaker (Manganese heptoxide) - NurdRage
- Nickel 'peroxyde'(s) - ChemPlayer
- Chlorine oxides
  https://en.wikipedia.org/wiki/Chlorine_oxide
- KO2: Potassium superoxide. Chemical oxygen generator. - ChemicalForce
- Perchloric acid
  perchloric-acid
  - HClO4 from NH4ClO4 (no distillation, simple elimination of ammonium) - Laboratory of Liptakov
  - Much simpler : distillation of perchlorate salt + sulfuric acid
- L'eau de Javel : fabrication, propriétés (graphs de durée de vie, potentiels-pH, espèces présentes suivant le pH...), utilisations - BULLETIN DE L’UNION DES PHYSICIENS
- Making high conc. Permanganate by Manganese electrolysis - Scrap Science
- Liquefying NO2/N2O4 (Dinitrogen tetroxide)
- Periodinane de Dess-Martin
  https://fr.wikipedia.org/wiki/Periodinane_de_Dess-Martin
- Peracetic acid
  peracetic-acid
  - Peracetic acid
    https://en.wikipedia.org/wiki/Peracetic_acid
  - Oxidations : Peracetic acid
    https://www.organic-chemistry.org/chemicals/oxidations/peracetic-acid.shtm
- Make Potassium Permanganate - NurdRage
- Dichlorine Hexoxide - this liquid EXPLODES on laser beam exposure! - ChemicalForce
- This Candle MAKES Oxygen and Started a Fire on a Space Station - NurdRage
- An Interesting Oxidizing Agent: Potassium Ferrate - Thy Labs
- Making Lithium Peroxide - NileRed
Solvants, extractions
solvants-extractions
- How to Best Dry Solvents - That Chemist
- Distillation of Gasoline - Extractions&Ire
- Extracting Pentanes & Hexanes from Gasoline - Extractions&Ire
- Making Solvents from Gasoline - Chemiolis
- Preparing a Drying Agent (anhydrous magnesium sulfate) - NileRed
- Chloroform
  chloroform
  - Preparation of Chloroform [with mechanism expl.] - UC235
  - Make chloroform by the haloform reaction - NurdRage
  - Chloroform by the haloform reaction - ChemPlayer
  - Chloroform by the haloform reaction (bleach+acetone) - Doug's Lab
- Making Isopropyl Nitrite - Doug's Lab
- 1,1,1-Trichloroethane
  https://en.wikipedia.org/wiki/1,1,1-Trichloroethane
- 1,1-Dichloroéthane
  https://fr.wikipedia.org/wiki/1,1-Dichloro%C3%A9thane
- Chloroéthane
  https://fr.wikipedia.org/wiki/Chloro%C3%A9thane
- CS2: Carbon disulfide. Chemical reactions - ChemicalForce
- Diethyl ether
  diethyl-ether
  - Diethyl ether - Sciencemadness Wiki
    http://www.sciencemadness.org/smwiki/index.php/Diethyl_ether
  - Dehydration of ethanol to ether - Frank Harrison
    https://yarchive.net/chem/ether_make.html
  - Ether For Anesthesia - MassGeneralHospital
  - Making Diethyl Ether - NileRed
  - Make Diethyl ether - myst32YT
  - Diethyl Ether Synthesis - ChemX
  - Purifying and Drying Diethyl Ether For Grignard Reactions Using Potassium Hydroxide and Sodium - NurdRage
- How to extract Cinnamaldehyde from Cinnamon - NileRed
- Potassium Metal From Bananas! - Cody'sLab
- Dioxane
  dioxane
  - Cubane Ep 5 - Dioxane and Bromine [chlorine-free Br2 with H2O2] - Extractions&Ire
- Essences hydrocarbures (A,B,C,E,F,G,H) - scienceamusante.net
  https://wiki.scienceamusante.net/index.php?title=Essences%20hydrocarbures
- Petroleum ether = Éther de pétrole = Ligroïne = Essence G = Naphta léger
  https://en.wikipedia.org/wiki/Petroleum_ether
- Making 1,3-Dioxolane - Chemiolis
Alcools
alcools
- From Sugar to Anhydrous Ethanol - ElementalMaker
- Phenol from Salicylic Acid (thermal decarboxylation) - Doug's Lab
- How to make anhydrous ethanol (100% alcohol) - NileRed
- How is propane converted into propanol? - Quora
  https://www.quora.com/How-is-propane-converted-into-propanol
- Alcools de fusel -> isomères de butanol, hexanol, alcool amylique, propanol...
  https://fr.wikipedia.org/wiki/Alcools_de_fusel
- Benzyl alcohol and benzoic acid from skin lotion - ChemPlayer
- Using the Grignard Reaction to Make Tertiary alcohols - NurdRage
Esters
esters
- Make Ethyl Propionate by Fischer Esterification - NurdRage
- How to make acetate esters with acetylation (acetic anydride) - NileRed
Ethers
ethers
- Williamson ether synthesis
  https://en.wikipedia.org/wiki/Williamson_ether_synthesis
- Diethyl ether
  diethyl-ether
Divers
divers
- The Final Steps of Making Pyrimethamine ("Daraprim") - NurdRage
- Sodium-Mercury amalgam - NileRed
- Ammonium-Mercury amalgam - NileRed
- The Chemical Adventures with Bicyclobutane
  http://ccc.chem.pitt.edu/wipf/Topics/Maciej.pdf
- Making uranium glass - NileRed
- Oxidizing and reducing flames
  https://en.wikipedia.org/wiki/Oxidizing_and_reducing_flames
- Eating the alkali metals : Salts taste test
- Make PCB Tinning Solution ("Liquid Tin") by Redox Flipping - NurdRage
- Carbon Monoxide generated from H2SO4 and formic acid - Doug's Lab
- Benzoyl peroxide Free-Radical polymerization of Methyl acrylate - ChemicalForce
- Emulsion Polymerization - Making Polymer Nanoparticles - RACInational
- Environemental impact (and composition) of used motor oil - Vazquez & Duhalt 1989
- Extracting urea from my own pee - NileRed
- Chemical exhibit: White flames - Rhodanide
- Hypophosphorous acid decomposition : a (toxic) firework - Rhodanide
- SOCl2: Thionyl chloride - ChemicalForce
- Pyrophoric gases : Silane and Diborane - Explosions&Fire and ChemicalForce
- Hazel Chem pyrolysis reactors
  pyrolyse
  - recycling of polystyrene / synthesis of styrene - Hazel Chem
  - polystyrene recycling part 2 (fractional vacuum destillation) - Hazel Chem
  - plastic waste to gasoline pyrolytic recycling - Hazel Chem
  - purification of pyrolysis oil - Hazel Chem
  - deacidifying pyrolysis oil / extraction of naphthenic acid from synthetic oil - Hazel Chem
  - how to make a plastic waste to fuel pyrolysis reactor - Hazel Chem
  - plastic waste to oil/fuel improved pyrolysis reactor - Hazel Chem
  - pyroylsis reactor project update - Hazel Chem
  - pyrolyis reactor update 2 (glue problem fixed) - Hazel Chem
  - pyrolysis reactor update 3 - Hazel Chem
- [Alcool production] Methanol Part 1 : where it comes from during fermentation - StillBehindTheBench
- [Alcool production] Methanol Part 2 : distillation (gets into the tails when pot-distilling, gets into the heads when frac-distilling) - StillBehindTheBench
- Making aluminum isopropoxide - NileRed
Divers inorganiques
divers-inorganiques
- Nickel chloride NiCl and boride from NiCO₃ - ChemPlayer
- Synthesis of Copper monosulfide with Hydrogen sulfide - Rhodanide
- Synthesize Copper Compounds - TheHomeScientist
- Synthesize Ammonium Metavanadate - TheHomeScientist
- SbCl3 Synthesis and Distillation (Short-path) - Extractions&Ire
- Synthesis of Copper Phthalocyanine - Texium
- Ionic liquids for energy storage and conversion - chemicum
- Making the Pharaoh's Serpent - NileRed
- Lead (II) chloride PbCl2 to recover lead from failed PbAc2 synthesis - Hazel Chem
- Sabatier reaction (methane from CO2 and H2)
  https://en.wikipedia.org/wiki/Sabatier_reaction
- Mixing Alkali and Chlorinated Solvents (Potassium and Carbon Tetrachloride explosion) - Explosions&Fire
- Extracting Cadmium from a NiCd Battery : HNO3 dissolution, sulfide precipitation - Extractions&Ire
- Copper and iron chemistry : around etchants
  copper-chemistry-around-echants
  - Make 10 Etchants for Copper Printed Circuit Boards - NurdRage
  - Make Ferric Chloride (for etching printed circuit boards) - NurdRage
  - Make Copper Chloride (3 ways) - NurdRage
  - Recover Copper from Ferric Chloride Etchant (Waste free method) - NurdRage
  - Recycle Copper chloride PCB etchant (waste free method) - NurdRage
  - Make an Air Sensitive Solution - NurdRage
- Make Silver Acetate - NurdRage
- Make pure MnO2
  make-pure-mno2
  - 1) Make MnSO4 from MnO2 [2 ways : SO2; oxalic/sulfuric acids] - NurdRage
  - 2) Purification of Manganese Sulfate from iron impurities - NurdRage
  - 3) Make Manganese Dioxide (MnSO4 + KHSO5 approach) - NurdRage
- From Thorium Hydroxyde to Thorium Chromate - Rhodanide
- Synthesis of Tin Tetraiodide - Rhodanide
- OZONIDES! Potassium and Cesium Ozonides. KO3, CsO3 - ChemicalForce
- Ammonium ozonide - ChemicalForce
- Experiment No. 30: Preparation and properties of Potassium nitrite (formate-method without any lead) - Experimental Chemistry
- Iron pentacarbonyl
  https://en.wikipedia.org/wiki/Iron_pentacarbonyl
- Uranium Metal From Ore (via ammonium, yellow cake and hexafluoride) - Cody'sLab
- Lab Notes : Failure in Making Sodium Nitrite (metabisulfite SO2 generator -> SO2 + dry nitric acid -> nitrosylsulfuric acid -> isopropyl nitrite from isopropanol -> sodium nitrite; only the last step is a failure, the rest works great) - NurdRage
- Make Isopropyl Nitrite without Sodium Nitrite - NurdRage
- Selenium chemisty. Red-Black Transformations - ChemicalForce
- Selenic acid, a very strong oxydizer - ChemicalForce
Transition metal chemistry, complexes
transition-metal-chemistry-complexes
- Making a Carbonato-Ammine-Cobalt Complex [Co(NH3)4CO3] - Extractions&Ire
- More Carbonato-Transition metal complexes - Extractions&Ire
- BNCP - bis-nitrotetrazolato-tetramine-cobalt perchlorate
  bncp
- Iron Heart Bleed (FeSCN)
  complexation
  - Make an Iron Heart Bleed (chemistry trick) (FeSCN) - NurdRage
  - Make Iron BLEED - NurdRage
- Copper tetraammine sulfate (complex) preparation - ChemPlayer
- Make Conductive Silver Ink (complex ion based) - NurdRage
- Separating Cobalt From Nickel (Cobalt From Li-ion Batteries - Part 4) - Scrap Science
- How Does Aqua Regia Dissolve Gold and Platinum? - NurdRage
Reductions and Reducing agents
reducing-agents
- Sodium thiosulfate preparation from sodium sulfite and sulfur - ChemPlayer
- White phosphorus from red phosphorus - woelen
  https://woelen.homescience.net/science/chem/exps/RedP2WhiteP/index.html
- How to Make White Phosphorus | Extended version - Aussie Chemist
- Hypophosphorus acid preparation (for alcohol -> alcane reduction) - ChemPlayer
- Phenylacetic acid synthesis (from mandelic acid via H3PO2 red.) - ChemPlayer
- Reduction of benzylic alcohols and α-hydroxycarbonyl compounds by hydriodic acid in a biphasic reaction medium
  https://www.beilstein-journals.org/bjoc/articles/8/36
- A hydrogen sulfide generator using... a candle : wax+sulfur->H2S - Extractions&Ire
- Reduction of Vanillin to Vanillyl Alcohol by BH4/borohydride - Rhodanide
- Sodium Borohydride NaBH4 Reduction Reaction Mechanism - Leah4sci
- GeH4: Germane - ChemicalForce
Agents halogénés
agents-halogénés
- Interhalogen compound: ICl3 Iodine trichloride - ChemicalForce
- Experiments with iodine monochloride (interhalogen compound) - ChemicalForce
- Synthesis of Phosphorus Tribromide - Texium
- Organic Hypochlorites : methyl/ethyl hypochlorite - Sciencemadness
  http://www.sciencemadness.org/talk/viewthread.php?tid=1896#pid29959
- Dichlorine Hexoxide (synthesis from ozone and ClO2 and explosive experiments) - ChemicalForce
- PCl3 and PCl5, PBr3 and PBr5
  pcl3-and-pcl5
  - Sometimes, bromides can be used in place of chlorides (it's easier and safer to handle)
  - Phosphorus trichloride - Sciencemadness Wiki
    http://www.sciencemadness.org/smwiki/index.php/Phosphorus_trichloride
  - The most convenient route involves the reaction of white or red phosphorus with chlorine, in PCl3. The PCl3 solvent where the bulk process takes place is made by reacting dry chlorine with phosphorus directly, and then more dry phosphorus is added, followed by the addition of dry chlorine. The reaction takes place under reflux and the resulting phosphorus trichloride is fractionally distilled to prevent the formation of PCl5.
  - PBr3 from bromine and red P - woelen
    https://woelen.homescience.net/science/chem/exps/PBr3_synth/index.html
  - There is an equilibrium PCl5 <-> PCl3 + Cl2, so P + PCl5 -> PCl3 should work by adding excess red P
  - Phosphorus trichloride - sciencemadness
  - Making phosphorus pentachloride PCl5 - THYZOID LABORATORIES
- N-Bromosuccinimide
  https://fr.wikipedia.org/wiki/N-Bromosuccinimide
- VCl4 from Vanadium metal and Chlorine - Extractions&Ire
- Sulfur chlorides
  sulfur-chlorides
  - Sulfur Monochloride (Disulfur Dichloride) - Doug's Lab
  - Making awful Sulfur Chlorides from Sulfur - Extractions&Ire
  - Sulfur dichloride - Sciencemadness Wiki
    http://www.sciencemadness.org/smwiki/index.php/Sulfur_dichloride
  - Sulfur dichloride synthesis - James Cambell
Composés halogénés
composés-halogénés
- Ethanol chlorination - Sciencemadness
  http://www.sciencemadness.org/talk/viewthread.php?tid=3919
- How To Make Isobutyl Bromide (Red P and Br2 Method) - Jupiter Chemistry
- How to make Chloroacetone - NileRed
- 2,4,6-trichlorophenol
  2-4-6-trichlorophenol
  - Fiche INERIS : détails sur la fabrication, la purification, la toxicité et les impuretés
  - NurdRage : If you're going to make trichlorophenol please be careful and thoroughly research the formation of side products like TCDD. I wanted to make TCP awhile back but i decided against it due to TCDD formation. [après quelques recherches, ça a l'air de concerner la fabrication du 245-TCP, pas du 246-TCP]
  - Dioxines dans l'environnement : rapport de l'INSERM -> détails sur le Réarrangement d’Ullmann (p23) responsable de la formation des dioxines à partir des chlorophénols
- Synthesis of a Bromoalkane (n-Bromopropane) - NileRed
- Bromoethane / Ethyl Bromide Synthesis - ChemX
- Purification and Drying of Ethyl Bromide - ChemX
- Make Alkyl Halides Bromoethane and Bromohexane - NurdRage
- Make Ethyl Bromide (Bromoethane) - myst32YT
- Methods of Chlorination of Primary non Benzylic Alcohols (without SCl2) - Sciencemadness
  http://www.sciencemadness.org/talk/viewthread.php?tid=2726
- Ethyl bromide / chloride : p71 of "THE PREPARATION OF ORGANIC COMPOUNDS", Barnett
- An Efficient Route to Alkyl Chlorides from Alcohols Using the Complex TCT/DMF
- Chloroacetic acid & cie.
  chloroacetic-acid
  - Synthesis of Chloroacetic Acid (direct chlorination of acetic acid, not very good...) - Hazel Chem
  - Synthesis of chloroacetic acid (direct chlorination of acetic acid, quite good) - MADscienceMAX
  - Acide trifluoroacétique
    https://fr.wikipedia.org/wiki/Acide_trifluoroac%C3%A9tique
  - Chloroacetic acid - Sciencemadness Wiki
    http://www.sciencemadness.org/smwiki/index.php/Chloroacetic_acid
  - Synthesis of chloroacetic acid - Rhodium site archive
    https://www.erowid.org/archive/rhodium/chemistry/chloroacetic.html
  - Direct chlorination of acetic acid produces a mix of mono,di,tri-choloracetic acid, which is a pain to separate
- Synthesis of chloral hydrate - Hazel Chem
- Process for the preparation of oxalyl chloride (with hosphorus pentachloride) - US Patent 4341720
- Making Methyl Iodide - NileRed
- Chlorinating C2Cl4 to C2Cl6 (hexachloroethane) - Doug's Lab
- Stinky, smoky orange stuff : Tetrabromoethylenediamine (bromination of ethylenediamine by hypobromite) - Rhodanide
- Chlorobutanol synthesis from acetone and chloroform - NCCHEM
- Chlorobenzene from benzene and NaDCC - Hydrogen, Time
- Preparation of chlorobenzene from sodium dichloroisocyanurate (NaDCC)
- Isopropyl chloride (2-chloropropane) from isopropyl alcohol, hydrochloric acid and calcium chloride - OrganoLeptic
- Benzyl chloride (α-chlorotoluene) and benzal chloride (α-dichlorotoluene)
  benzyl-chloride
  - Benzyl chloride
    https://en.wikipedia.org/wiki/Benzyl_chloride
  - Benzyl chloride - Sciencemadness Wiki
    http://www.sciencemadness.org/smwiki/index.php/Benzyl_chloride
  - Photochemical reaction of toluene with chlorine (produces a mix of α-{mono,di,tri}chlorotoluene which is difficult to separate)
  - Blanc chloromethylation (benzene + formaldehyde -> benzyl chloride)
    https://en.wikipedia.org/wiki/Blanc_chloromethylation
  - Benzyl alcohol + HCl -> benzyl chloride (nicest route)
  - Making Benzyl Chloride (from benzyl alcohol) - NileRed
  - Synthesis of benzyl chloride (from benzyl alcohol) - chemx01
  - Synthesis Of Benzyl Chloride from Benzyl Alcohol - Full Modern Alchemist
  - Sciencemadness Discussion Board - Benzyl and Benzal chloride, Benzaldehyde and Benzoic Acid - Illustrated Practical Guide
    http://www.sciencemadness.org/talk/viewthread.php?tid=10256
  - Making benzal chloride - Toluene photochlorination - Ilusys Systems
  - Synthesis of benzyl chloride by the free radical chlorination of toluene using TCCA - OrganoLeptic [very nice, clean, 30% yield on TCCA]
- Allyl Alcohol and Allyl Bromide From Pineapple Perfume - LabCoatz
Organiques simples
organiques-simples
- Styrene by polystyrene depolymerization, and synthesis of Styrene Dibromide - UC235
- Making 1-MCP series : isobutene from tert-butanol, chlorination of isobutene to methalyll chloride, ... - Extractions&Ire
  making-1-mcp-extractions-ire
  - Making Apples Immortal with 1-MCP - Project Intro - Extractions&Ire
  - Elimination of tert-Butanol with Sulfuric Acid - Extractions&Ire
  - Chlorination of Isobutene in liquid phase [fail] - Extractions&Ire
  - Chlorination of Isobutene in gas phase [fail] - Extractions&Ire
  - Chlorination of Isobutene in gas phase [attempt 2, fail] - Extractions&Ire
- Synthesising Cyclopentanone through Catalytic Decarboxylation of Adipic acid - Extractions&Ire
- Nitrites d'alkyle
  nitrite-d-alkyle
  - Isopropyl Nitrite
    isopropyl-nitrite
    
    Isopropyl Nitrite - Doug's Lab
- Gattermann-Kock reaction
  https://en.wikipedia.org/wiki/Gatterman-Koch_reaction
- Phenyl 2 propanone (P2P) from acetone, bromine and benzene - ChemPlayer
- Sulfonation: p-Toluenesulfonic Acid - Doug's Lab
- Dimethyl Oxalate - Doug's Lab
- Pyridine
  pyridine
  - Pyridine from Niacin - Doug's Lab
  - How to make Pyridine from Vitamin B3 (+ copper chromite cat.) - Extractions&Ire
  - Preparation of Pyridine - magpie - Sciencemadness Discussion Board
    http://www.sciencemadness.org/talk/viewthread.php?tid=13130
  - Copper chromite
    copper-chromite
- Succinimide from Succinic acid - Extractions&Ire
- The Cannizzaro reaction (benzaldehyde -> benzyl alcohol + benzoic acid) - NileRed
- Alkyl borates
  alkyl-borates
  - Preparation of Trimethyl Borate //[have B(OMe)3 in MeOH, last purification step here]// - Magpie, Science Madness
    http://www.sciencemadness.org/talk/viewthread.php?tid=16439
  - Preparation and Purification of Methyl Borate and Ethyl Borate - Webster, 1933
  - Procedures for the Preparation of Methyl Borate - Schlesinger, 1953
- CHCl3 and CCl4 Prep Overview (chloral, trichloroacetic, MeSCN routes) - Sciencemadness
  https://www.sciencemadness.org/whisper/viewthread.php?tid=10300
- Turning Styrofoam into Benzoic Acid - Chemical recycling of polystyrene - MADscienceMAX
- Benzène
  benzène
  - Preparation of benzene, compiled by CHROMIUM, ScienceMadness
    http://www.sciencemadness.org/member_publications/benzene_production.pdf
  - Synthesis of Benzene (CaO as oxydizer) - PbN32
- Synthesis of ortho para nitrotulene - Hazel Chem
- How to Convert Aspirin (Acetylsalicylic acid) to Salicylic acid (Base Hydrolysis Method) - NileRed
- Turning Aspirin into methyl salicylate in a one-pot reaction (transesterification) - NileRed
- Making methyl salicylate (wintergreen, a minty odor and flavoring) - NileRed
- Hydrazine
  hydrazine
  - Make Hydrazine Sulfate by the Hypochlorite-Ketazine Process - The Complete Guide - NurdRage
  - Hydrazine sulfate (urea+bleach) - Tetrazoles Part 4 - Extractions&Ire
  - Hydrazine sulfate v2 - Extractions&Ire
  - Making Hydrazine Sulfate from Urea and Bleach - NileRed
  - Synthesis of Hydrazine Sulfate: Part 1 - UC235
  - Synthesis of Hydrazine Sulfate: Part 2 - UC235
  - Azeotropic hydrazine synthesis (from urea+bleach) - Pyrotechnical
- Preparation of Mononitrotoluenes (o-, p-) - Sciencemadness
  http://www.sciencemadness.org/talk/viewthread.php?tid=29111
- Making Acetylacetone - ReactiveChem
- Making Sodium Ethoxide and Prepping Solvents for Acetylacetone - ReactiveChem
- Making Cinnamic Acid - NileRed
- Making Oxetane - Chemiolis
- Allyl Alcohol and Allyl Bromide From Pineapple Perfume - LabCoatz
- Making Benzilic Acid (hydroxy diphenyl acetic acid) from benzil (diphenylethanedione) in two ways - Thy Labs
- The Étard reaction : oxydizing toluene to benzaldehyde with chromyl chloride - NileRed
- The Étard reaction : oxydizing toluene to benzaldehyde with chromyl chloride (better yield than NileRed but still shit) - Chemiolis
Divers organiques
divers-organiques
- Cyclisations
  cyclisations
  - Synthesis of 3,5-Dimethylpyrazole - Corrosive Chemistry
  - Knorr Pyrrole Synthesis of Knorr's Pyrrole - Corrosive Chemistry
  - Making [1.1.1]Propellane - Chemiolis
- Perthiocyanic Acid - Yellow Chem GOOD! - Rhodanide
- Claisen condensations
  claisen-condensations
  - Trans cinnamic acid synthesis via claisen condensation (part 1) using benzaldehyde and ethyl acetate - Hazel Chem
  - Cinnamic acid synthesis part 2 (ethyl ester hydrolysis) - Hazel Chem
  - Synthesis of Ethyl Acetoacetate (Claisen condensation of ethyl acetate) - UC235
- Extraction/recrist of dibenzoyl peroxide - Hazel Chem
- Extraction of piperine from white pepper - Hazel Chem
- How to make cadaverine (the smell of death) - decarb of lysine - NileRed
- Controlling phenolic hydrodeoxygenation by tailoring metal-O bond strength via specific catalyst metal type and particle size selection
- Diethylamine and m-toluic acid from DEET
- Alkynes as Synthetic Equivalents of Ketones and Aldehydes: A Hidden Entry into Carbonyl Chemistry
- Turning cotton balls into cotton candy : depolymerization of cellulose to glucose by sulfuric acid - NileRed
- Preparation of toluene and (de)sulfonation in detail - Astral Chemistry
- Sucrose Octaacetate Synthesis, An Intensely Bitter Compound - Corrosive Chemistry
- Experiment No. 25: Preparation of Ethene (without conc. sulfuric acid) & detection with Bayer's test - Experimental Chemistry
- Making the stinkiest chemical known to man (thioacetone) - NileRed
- Making Thioacetone - LabCoatz
- US government standard bathroom malodor - NileBlue
- Making the Smell of Rain (Geosmin from scratch) - Chemiolis
- Acetone ---dehydration--> mesitylene (1,3,5-trymethylbenzene) ---nitration--> nitromesitylene ---béchamp(Fe,HCl)-reduction,acid-base-extraction--> trimethylaniline ---oxydative-azo-coupling---> azomesitylene (red azo dye), with lots of interesting purification techniques - Chemiolis
- Cubane chemistry
  cubane-chemistry
  - Cubane synthesis - Extractions&Ire
    cubane-synthesis
    
    Many interesting techniques in this series : recrystalizations, purifications, TLCs with various detection methods (permanganate, iodine, UV, vanillin), contamination mitigation, quite cold temperatures, reaction times, decomposition, photochemistry, protection/deprotection, water-free techniques, tar management...
    
    Project plan: Cubane synthesis - Extractions&Ire
    
    Synthesising Cyclopentanone through Catalytic Decarboxylation of Adipic acid - Extractions&Ire
    
    Cubane Episode 2 - Cyclopentanone Ketal [failure : aldol condensation] - Extractions&Ire
    
    Cubane Episode 3 - Vacuum Distillation for the Ketal? [failure] - Extractions&Ire
    
    Mastering the Ketal Synthesis [or how to avoid aldol cond.] - Cubane Episode 4 - Extractions&Ire
    
    Cubane Ep 5 - Dioxane and Bromine [chlorine-free Br2 with H2O2] - Extractions&Ire
    
    Bromination of the ketal - Cubane Episode 6 - Extractions&Ire
    
    The Diels-Alder - Making Cubane Episode 7 - Extractions&Ire
    
    Cubane Ep 8 - Deprotection Time! Diketal to monoketal [in heterogeneous mixture, HCl]. TLC stuff. - Extractions&Ire
    
    Cubane Ep 9 - *Actually* forming the MonoKetal. Amazing NMR results - Extractions&Ire
    
    Cubane Ep 10 - Ultraviolet Cage Creation [failure] - Extractions&Ire
    
    Cubane Ep 11 - More UV Nightmares [failure, more TLC nightmares] - Extractions&Ire
    
    Cubane Ep 12 - Magical deep UV LEDs [failure] - Extractions&Ire
    
    Cubane Ep 13 - The PhotoFridge [failure] - Extractions&Ire
    
    A slightly new cube plan... [UV sensitization, litterature review, progress by others] - Cubane Ep 14 - Extractions&Ire
    
    I lost the cubane race (Still going though!) [new plan : no monoketal intermediate, doing the photoreaction directly on the diketone; resynthesis and purification of reagents] - Cubane Ep. 15 - Extractions&Ire
  - Cubane synthesis - Chemiolis
  - Cubane synthesis - Lumiray
    cubane-synthesis-lumiray
    
    Cyclopentanone ketal - Lumiray
- Synthesis of a Fascinating Cube-Shaped Molecule : Octasilacubane - Advanced Tinkering
- Making Bromovanillin: A Precursor To Substituted Benzaldehydes - Thy Labs
- Making margarine from olive oil - NileRed
- Olestra (zero calorie cooking oil) - chemical synthesis and taste test - Applied Science
- Turning Aspirin into Paracetamol (acetyl salicylic acid --> salicylic acid ---decarb--> phenol ---nitration--> p-nitro phenol ---P/C reduction--> p-amino phenol ---acetylation--> p-acetylamino phenol) - NileRed
- Making Rose Fragrance from Lemongrass : citral ---aldol cond. with acetone---> ---cyclization--> ionone - Chemiolis
Métaux alcalins
métaux-alcalins
- How to make caesium - olympicfan2
- Isolating Cesium Metal - Cody'sLab
- Making Potassium Metal - Cody'sLab
- Cody's Alkali Metal Converter - Cody's Lab
- unused footage from "cody's alkali metal converter" video made into another video - Cody'sBLab
- Domaine d'inertie électrochimique -> carbonate de propylène : -3.2 -> +3.5V
- Making Cesium on a Barbecue - Thunderf00t
- Fun with Rubidium - ChemicalForce
- Electrolysis of an alkali chloride salt disolved in propylene carbonate
- Sciencemadness Discussion Board - unconventional sodium
  http://www.sciencemadness.org/talk/viewthread.php?tid=2105
- Making Sodium Metal : The Castner Process (Electrolysis of NaOH) - Scrap Science
- Making Lithium Metal (Electrolysis of molten LiCl) - Scrap Science
- Making Calcium Metal (Electrolysis of molten CaCl2) - Scrap Science
- Sodium-Potassium Alloy: Blue Solvated Electrons in Water! - ChemicalForce
- A Non-Exploding Alkali Metal Drop on Water : From Blue Solvated Electrons to Bursting Molten Hydroxide (P. Mason et al.)
- Making cesium from CsCl - Advanced Tinkering
  making-cesium-from-cscl
  - Making cesium and distilling it in my homemade still - Advanced Tinkering
  - Making large quantities of very pure cesium by double distillation (Li+CsCl) - Advanced Tinkering
  - “How Much Cesium Do You Need?” – “Yes!” - Advanced Tinkering
- Gorgeous large-scale potassium distillation - Advanced Tinkering
- Combining what shouldn't be combined: Making Cesium superoxide - Advanced Tinkering
- Making Rubidium metal - Advanced Tinkering
- NaK MHD fountain – Periodic Videos homage - Advanced Tinkering
- Why you should never heat Lithium in glassware : reduces SiO2/glass to silicon ! - Advanced Tinkering
- Potassium Metal From Potash - Elias Experiments
- How I Mass Produced Potassium Metal In The Backyard (>1kg) - Elias Experiments
- Make Sodium Magnesium Oxide Aggregate (Mg/NaOH fire) - NurdRage
- Make Sodium Metal with the High Temp Reduction Method (Mg/NaOH fire) and Dioxane Separation - NurdRage
- Nurd Rage lab notes : making sodium metal with the alcool-catalysed reduction method
  nurd-rage-lab-notes-making-sodium-metal
  - Using the Grignard Reaction to Make Tertiary alcohols - NurdRage
  - Vlog April 2018 - Failed experiments and work in progress on making alkali metals - NurdRage
  - Rushed Vlog May 9th - Sodium Discovery and Youtube Strike - NurdRage
  - Theory Test for Alcohol Catalyzed Magnesium Reduction of Sodium - NurdRage
  - Succesful Sodium Production with Inexpensive Chemicals and Continuing Optimizations - NurdRage
  - Lab Notes - Sodium progress report and dimethyl dioxane troubles - June 2018 - NurdRage
  - Lab Notes - Optimizing sodium, making HBr, and The Clevenger - NurdRage
  - Lab Notes - Alternative glassware protection for sodium production : Lithium drying and Aluminum drying <- - NurdRage
  - Lab Notes - Testing Alternative Catalysts for Making Sodium - NurdRage
  - Lab Notes - Unrefined tea tree oil tests and stoichiometry tests - NurdRage
  - Lab Notes - Purified Tea Tree Oil Experiments for Making Sodium - NurdRage
  - Lab Notes - Terpin Hydrate failures, Urushibara Nickel failure, and Additional Sodium Work - NurdRage
  - Lab Notes - Off the Shelf Catalyst Testing - Nov 11th 2018 - NurdRage
  - Lab Notes - Fundamental Mechanistic Insight and New Catalysts for Making Sodium - NurdRage
  - Lab Notes - Eucalyptol Testing (Fail) - NurdRage
  - Make Sodium Metal with Menthol-catalysed reduction method - NurdRage
  - Lab Notes - trying to make lithium (and failing) - NurdRage
- Make Sodium Metal with Menthol-catalysed reduction method - NurdRage
Catalyseurs
catalyseurs
- Preparation of elemental Cobalt - Rhodanide
- Copper(I) chloride
  https://en.wikipedia.org/wiki/Copper(I)_chloride
- Preparation of CuCl from metal copper and CuCl2 - Rhodanide
- Copper (I) chloride preparation using hypophosphite - ChemPlayer
- Copper chromite
  copper-chromite
  - Copper Chromite Catalyst (for decarboxylation) - Doug's Lab
  - Copper chromite
    https://en.wikipedia.org/wiki/Copper_chromite
Metal refining
metal-refining
- Palladium recovery from 1.4kg ceramic capacitors - OwlTech
- Make Purified Chloroplatinic Acid - NurdRage
- Make Gold from Chloroauric Acid - NurdRage
- Gold Coin Dissolving in Acid (Aqua Regia) - NurdRage
- Pepto Bismol as a fire assay lead replacement - Cody'sLab
- Making purple gold (Al2Au alloy) - NileRed
- Li-ion battery extractions (Li, Co, Ni, Mn...)
  li-ion-battery-extraction
  - Lithium From Li-ion Batteries - Part 1 - Scrap Science
  - Lithium From Li-ion Batteries - Part 2 - Scrap Science
  - Cobalt From Li-Ion Batteries - Part 3 - Scrap Science
  - Separating Cobalt From Nickel (Cobalt From Li-ion Batteries - Part 4) - Scrap Science
Électrochimie
électrochimie
- How to properly copper plate steel (nickel coating) - Pyrotechnical Science
- Restoring Lab Oven via Zinc Plating (portable zinc plating !) - Aussie Chemist
- Make Silver Powder by Electrochemistry - NurdRage
- Make a rechargeable Ag₂O/Zn Battery - NurdRage
- Electrochemical synthesis of perbromate using conductive-diamond anodes
- Make an AA alkaline battery (Zn, MnO2) - NurdRage
- Make a Zinc Air Battery - NurdRage
- Make pure MnO2
  make-pure-mno2
- Make Manganese Dioxide Electrodes - NurdRage
- Make an Aluminum Air Battery - NurdRage
- Grow Silver Metal Crystals by Electrochemistry - NurdRage
- TiO2/Raspberry based solar cell - NurdRage
- How to galvanize metal (zinc plating) - NurdRage
- Turn Pennies Silver and Gold (zinc plating on copper, then brass formation) - NurdRage
- The Electrolysis Of Urea - Scrap Science
- Making A Gas Diffusion Electrode - Scrap Science
- Making Sodium Metal : The Castner Process (Electrolysis of NaOH) - Scrap Science
- Make a Nafion Divided Membrane Cell for Electrolysis - NurdRage
- Make Sodium Hydroxide by Electrolysis with a Nafion Membrane Cell - NurdRage
Clock or oscillatory reactions
clock-or-oscillatory-reactions
- How to prepare the Iodine Clock Reaction - NileRed
- The Vitamin C Clock Reaction (reduction if iodine)
- Belousov-Zhabotinsky Oscillating Reaction - NileRed
- Liesegang rings
  https://en.wikipedia.org/wiki/Liesegang_rings
- On the dynamics of Liesegang-type pattern formation in a gaseous system (NH4Cl deposition in a tube)
  on-the-dynamics-of-liesegang-type-pattern-formation-in-a-gaseous-system
  - On the dynamics of Liesegang-type pattern formation in a gaseous system
    https://www.nature.com/articles/srep23402
  - Video 1 (raw video)
  - Video 2 (slow dynamics)
  - Video 3 (fast dynamics)
  - Video 4 (phase correlations)
  - Suppl. Info.
Techniques et matériel
techniques-et-matériel
- Aspirator Vacuum Pump Setup - NurdRage
- Lab Equipment: Short Path Distillation Apparatus - NurdRage
- Lab Equipment: The Clevenger Apparatus - NurdRage
- Chlorine and Gas Drying - Doug's Lab
- Sodium-Lead Alloy for (Safer) Solvent Drying. - UC235
- Making a Magnetic Stirrer Hotplate with an old kettle - Fereidoon Kavosian
- How to (not) clean Fritted Funnels
  http://www.ilpi.com/inorganic/glassware/frittedfunnel.html
- Piranha Solution great dangers
  https://yarchive.net/chem/piranha_solution.html
- Making thin-layer chromatography (TLC) plates - TheHomeScientist
- 2.3F: Visualizing TLC Plates - Chemistry LibreTexts
  https://chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_Lab_Techniques_(Nichols)/02%3A_Chromatography/2.03%3A_Thin_Layer_Chromatography_(TLC)/2.3F%3A_Visualizing_TLC_Plates
- Krytox PTFE grease
- Amateur Lab Equipment: Reverse Osmosis Deionization Systems for Purifying Water - NurdRage
- How to Regenerate Deionization Resin for Use in Reverse Osmosis Deionization Systems - NurdRage
- Molecular sieves; a must for drying ether
  https://yarchive.net/chem/molecular_sieves.html
- How to make a lab heating mantle - MADscienceMAX
- Making a genius gas flow back preventer that makes chemistry easier - MADscienceMAX
- Dealing with Stuck or Frozen Glass Joints
  http://www.ilpi.com/glassblowing/frozenglass.html
- The Scientific Glassblowing Learning Center: Home Page
  http://www.ilpi.com/glassblowing/index.html
- How to build a Pressure Cooker Pot Still (copper tubing build) - NileRed
- Huile minérale
  huile-minérale
  - Une huile minérale très peu aromatique ? Huile pour bébé hypoalergénique.
  - Huile de Vaseline Codex (qualité pharma, sans doute peu aromatique) - Mon-Droguiste.com
    https://www.mon-droguiste.com/huile-vaseline-clarifiee.html
  - Huile de Paraffine Industrielle (moins chère) - Mon-Droguiste.com
    https://www.mon-droguiste.com/huile-paraffine.html
  - Paraffine
    https://fr.wikipedia.org/wiki/Paraffine
  - En pharmacie : huile de paraffine
  - Aussi : huile de massage
  - Liquid paraffin (drug)
    https://en.wikipedia.org/wiki/Liquid_paraffin_(medicinal)
- Matos à acheter
  matos-à-acheter
  - Deschem
    deschem
    
    250ml Soxhlet Extractor Body (only, j'ai déjà le condenseur)
    
    Reducing adpater pour aller vers 24/29
    
    Glass thimble for Soxhlet extractor
    
    Un réacteur à couvercle pour se faire plaisir un jour (>100$)
    
    (Truc useless : Jacketed Glass Beaker)
    
    24/29 Lab Glass Distillation Receiver Adapter Clevenger Apparatus PTFE Stopcock | eBay
    https://www.ebay.com/itm/265570893570
    
    120ml Glass High Pressure Bottle,45*110 Heavy Wall Vessel With #15 PTFE Thred 6971311070843 | eBay
    https://www.ebay.com/itm/265557099159
    
    500ml,250W,Inner Sleeve use for 500ml Heating Mantle | eBay
    https://www.ebay.com/itm/262810027647
    
    24/29 Amber Glass Flask Round Bottom 1 Neck Lab Single-Neck Brown Boiling Bottle | eBay
    https://www.ebay.com/itm/265576972342?var=565369796249
    
    24/29,Distillation head Short Path Condenser,Glass Adapter,Lab Glassware | eBay
    https://www.ebay.com/itm/262819871362
    
    120mm,24/29,3-Way,Glass Vigreux Distilling Column,With Side Arm,Lab Glassware | eBay
    https://www.ebay.com/itm/262819785323
    
    24/29,Glass Thermometer Adapter,100mm Stem,Wide Open Mouth,Lab Glassware | eBay
    https://www.ebay.com/itm/262819768963
    
    200ml,24/29,Glass Buchner funnel,3# Coarse Filter,10mm Vacuum Hose,Lab Glassware | eBay (replacing the broken one)
    https://www.ebay.com/itm/262829589557
    
    500ml,3-Neck,24/29,Flat Bottom Glass Flask,Three Necks,Lab Chemistry Vessel | eBay
    https://www.ebay.com/itm/262792234475
    
    6 PCS New Magnetic Stirrer Mixer Bar,TYPE C PTFE Cover Stir Bar | eBay
    https://www.ebay.com/itm/262809673049
    
    2000ml,24/29,Glass Erlenmeyer Flask,2L,Chemistry Conical Bottle,Lab Glassware | eBay
    https://www.ebay.com/itm/262813050684
    
    170ml Glass High Pressure Bottle,45*150 Heavy Wall Vessel With #15 PTFE Thred 6971311070850 | eBay
    https://www.ebay.com/itm/265557099112
    
    25ml,Ground Joint Measuring Cylinder With Solid Stopper,Laboratory Glassware | eBay
    https://www.ebay.com/itm/262807270158
    
    1 more pipette
    
    24/29,Glass Straight Connecting Adapter,Cone and Socket,Laboratory Glassware | eBay
    https://www.ebay.com/itm/262819835178
    
    200mm,24/40,Glass Air Condenser,Lab Chemsitry Glassware | eBay
    https://www.ebay.com/itm/262784563253
  - New Distillation Head premium,Distillation head Short Path Condenser,24/40 | eBay
    https://www.ebay.com/itm/New-Distillation-Head-premium-Distillation-head-Short-Path-Condenser-24-40/233787570675?hash=item366ed339f3:g:KqcAAOSwz5hbsEh~
  - Hydrothermal Synthesis Autoclave Reactor Digestion Tank with PTFE Lined | eBay
    https://www.ebay.com/itm/313987337663
  - bouchons srew et rubber
  - glass spoon
  - 3A / 4A / 5A / 13X molecular sieve desiccant - AliExpress
    https://www.aliexpress.com/item/4000913031621.html
  - rubber scraper (tiny, for beakers)
  - 5x stopper 29/32
  - PU rubber
    pu-rubber
    
    Polyurethane liquid casting rubber Shore A 60 (Poly 75-60) - syntecshop.com
    https://syntecshop.com/en/polyurethane-liquid-casting-rubber-shore-a-60-poly-75-60
    
    Shore durometer
    https://en.wikipedia.org/wiki/Shore_durometer
  - DODECAVIT / B12a / hydroxycobalamine - for CN poisoning
    https://www.vidal.fr/medicaments/gammes/dodecavit-2944.html
  - TCL plates
  - precision pH paper
- Cyanide destruction methods
  https://www.sgs.pt/~/media/Global/Documents/Flyers%20and%20Leaflets/SGS-MIN-WA017-Cyanide-Destruction-EN-11.pdf
- How to Purify salts by water recrystallization - NurdRage
- Calcium chloride complexes alcools in addition to water : do not use to dry alcools !
- Utiliser un extracteur de Soxhlet pour des extractions de purifications/workups, genre trucs peu solubles dans l'hexane
Histoire
histoire
- The history of potassium/potash, blue ponds in the Utah desert - Veritasium
Chimie analytique
chimie-analytique
- Calcium and more metals (Sr,Ba..) from bones - Neptunium
- Measuring the amount of lead (Pb) consumed when drinking from lead crystal glassware. Is it safe? [Measuring many metals at µg/L concentrations with dithizone and a spectrometer] - Applied Science